At the beginning of the experiment, a number of things were noted that were expected to effect the progress of the two overlapping smelts:
1) The smelter structure had slumped forward slightly off vertical. This was largely due to the effect of damp conditions over the spring, softening the raw clay cobb that remained at the base of the structure. (From tuyere level up the clay had been converted to a rough ceramic by the three earlier firings.) It was also possible that the effect of frost heave on the half banked side of the smelter also contributed. The slight lean of the furnace towards the tap arch was not expected to have a significant effect on the progress of the smelts. The angle of the tuyere, which had remained in place after the two November firings, was a matter of concern. The angle had shifted from the ideal 22.5 degrees down to closer to 15 degrees down. In past experiments, a shallow tuyere angle has resulted in the slag bowl forming higher in the furnace, with more potential to quickly fill with slag and drown the tuyere. A smaller bloom is expected from a furnace with a shallow tuyere angle as well.
2) Most importantly, the rock iron ore was suspected to have a higher content of waste stone, and suspected also of being lower in iron oxide content as well. The rock ore remaining on hand was gathered by Darrell and Vandy from the secondary mine source discovered by Sauder and Williams. Although a day had been spent at the mine with the Lexington crew gathering ore, the material on hand had been gathered (and backpacked down off the mountain) by Darrell and Vandy working alone (and undirected) the following day. (Earlier Virginia Rock Ore used had been much better quality material gathered by Lee and Skip from their primary source.) When working without supervision, there had been a specific attempt made to gather ore with various differing physical appearance from a number of different locations within the overall deposit. This in the hope that the quality would average out in the end. During the crushing phase it was obvious that there was much more plain stone included inside the pieces gathered than had been present in past material.
The combination of these two factors suggested that the smelter would not only produce more glassy waste slag than had been the case in the past. Also it was expected that would also need more frequent tapping off of that same slag to prevent drowning of the tuyere. Overall it was expected that there would me significantly less available iron oxide, resulting in a smaller bloom and a lower total yield.
Our fuel source was once again Royal Oak Charcoal, supplied by yet a fourth kind donation of material from the company. (DARC thanks Royal Oak for its kind support by way of 600 pounds of charcoal which made this and future experiments possible.) Sam gets credit for crushing the bulk of the charcoal required for the two smelts using his impressive double mallet technique.
The first smelt was undertaken by Neil and Dr. Ron Ross, with Darrell guiding and troubleshooting (avoiding most of the work). Once finished with charcoal, Sam stepped in as record keeper over both smelts.
As is typical, although our intention was to start pre-heat for 8 AM, getting equipment set up and everything organized always delays the start, so actually the fire was started closer to 9:30. The preheat phase was fairly standard, with the switch to graded charcoal marking the official start of the smelt after 60 minutes. Over the first smelt the furnace ran evenly and maintained a textbook burn rate of 8 minutes per standard 4 lb charcoal charge. A total of 20 kg of ore was added for the first smelt. The course of the smelt followed what has come to be the fairly standard method : heat the stack / seed charges / main charges slowly increasing in volume / allow the last charge to settle then add a larger shock charge / burn down for extraction. (For detailed sequence, Neil is expected to publish the field data soon on to the DARC web site at www.darkcompany.ca/iron ) As was expected with the high rock ore, more glassy slag was created than in our past smelts, and several tappings were undertaken.
Neil prepared and started a top extraction. It was quickly clear that there was an excessive amount of liquid slag at tuyere level, and he was having trouble locating the potential bloom. His pounding with the thumper was found to be just splashing into a large pool of liquid slag. Darrell quickly stepped in (working without much gear on and burning off a glove in the process) and located and loosened out the smaller than expected bloom mass. Neil then grabbed it out with tongs and quickly moved it over to the consolidation stump, were Ron / Sam / Gus were waiting with large hammers. The bloom proved to be quite spongy, but was quickly worked down to a rough block a bit larger than fist sized. The finished bloom weighs only 900 gm. It still contains considerable slag and is expected to loose a significant amount of weight as it is later further compacted in the forge into a bar. The metal appears to be of workable quality however, expected to produce a good soft iron.
As soon as Neil moved out of the smelt area, the second team of Dave / Ken / Kevin got into action - the 'hot swap'. First the remaining ignited charcoal scooped from smelt one was dumped back into the furnace, with the remainder of stack filled with fresh charcoal and the air blast resumed. Because of the retained heat in the furnace, only one or two charging cycles were required to fully ignite the working height of the smelter and return to the desired 8 minutes per standard bucket burn rate. Again the standard ore charging sequence of seed charges / increasing volume of primary charges was undertaken.
Because the small size of the initial bloom had confirmed in our minds the low iron oxide content of the ore, it was decided to enrich the second smelt by adding hematite blasting grit. That material is over 90 percent iron oxide, but can often cause problems because of its actual lack of silica for slag formation. It was decided that mixing 50 % of the rock ore with 50% of the hematite might create a more balanced mixture of iron available inside the furnace. The method this team chose to employ was to alternate rock ore with hematite scoop by scoop, As the hematite is a bit more dense than the rock ore, the end result was slightly more of the hematite making up the roughly 25 kg total ore utilized over smelt two.
A significant secondary problem arose during the second smelt. The initial patching of the furnace wall in the tuyere area before the firing had been done with 'Blue Mountain Red' - a local ground clay which has a relatively low firing temperature. Soon into the second smelt, it was obvious that the smelter wall above the tuyere, but within the supporting earthen bank, had burned through. Dramatic slumps of the ash and sand packing mix on the tuyere side of the smelter indicated large amounts of this material was falling into the furnace. By keeping a quantity of this mix handy, it was possible to fill in the developing hole. Over the course of the second smelt the better part of a 20 litre pail of packing mix was consumed in this way. Mixing ash and sand and then bringing it to the kind of heat existing in the interior of a smelter (1100 C or more) results in the creation of glass. Huge volumes of light glassy slag were being produced from this source alone. Add that to the slag still in place from the first smelt, plus any new slag being formed from the addition of high rock content ore and it was obvious that slag volume was going to present a major problem. The team had to undertake a number of fairly large slag taps to keep the tuyere clear. Eventually the large volumes of glass being created via the packing mix (going through what latter proved to be a fist sized hole) started to block of the tuyere.
Although not quite ready to extract the bloom in terms of an ideal sequence, the relatively sudden restriction in air flow lead to the decision to pull the bloom. Because the smelter was not considered likely to be recoverable, it was suggested to make a bottom extraction through the tap arch. It proved difficult to pull out the bricks filling the tap arch, as repeated slag taps had created a large mass of solidified glass around them. Some close work with steel rod and hammer by Ken broke up and cleared the bricks and exposed the original base layer of charcoal fines and ash under the slag bowl. Kevin was then able to rake clear the bottom of the bowl. This was punctured, and hot liquid slag allowed to flow into the gap to soften the lower surface of the bowl. Next Dave was able to hammer clear some of the upper edges of the combined slag mass. Quickly moving to hook and pry at through the tap arch, the bloom popped free quite suddenly.
Again the bloom mass was moved over to the consolidation stump. With Dave / Ken / Sam on the hammers and Kevin holding, the loose mother was knocked clear and the ragged edges compacted. The bloom was returned to the smelter body for another heat to allow for a second compaction. The end result was a rough cube of metal with a total weight of about 3100 gms. The second bloom is considerably more dense, more in line with what would be expected in a successful smelt.
Although the yields are considerably less than what we have come to expect, this is consistent with suspected low iron content of the ore used. The improved efficiency of a double smelt was clearly illustrated in terms of both reduced time and lower overall charcoal consumption. Some further experimentation remains on designing a more durable smelter, but it is important to remember that the furnace used was undertaking its fourth and fifth repeat firing at this point with only minimal repairs. Overall the teams were able to predict and respond effectively to problems that arose over the course of each smelt event. There is no doubt that the overall confidence and ease of action of individual participants improved significantly over this experiment.
(Sunday's activities with Dr. Ross will be detailed in a separate post)
Dave Here.
ReplyDeleteWow you don't waste much time in posting, do you?
I consider this to be a sucsess, between responding to what the first bloom was telling us and an increased sense of understanding/control of the process on a deeper level
oh ya it was me on tongs first, then after the reheat Ken. All in all good Stuff
Neil Here,
ReplyDeleteTwo quick fixes, You extracted the bloom and controlled it for pounding during smelt #1 (you were extracting it at that point) -- I helped team two restart the smelter for smelt #2.
With bloom 2 I hammered during the first heat, and turned the hammer over to Kevin when he became available for the second set of hammering.
I'm with Dave -- I consider this to be a solid success on both smelts.
You should also comment on Dr. Ron's work mapping out the site on sunday.